Home Cart Sign in  
Chemical Structure| 167611-99-6 Chemical Structure| 167611-99-6

Structure of 167611-99-6

Chemical Structure| 167611-99-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 167611-99-6 ]

CAS No. :167611-99-6
Formula : C11H17NO4
M.W : 227.26
SMILES Code : O=C([C@@H]1[C@]2([H])C[C@]2([H])CN1C(OC(C)(C)C)=O)O
MDL No. :MFCD08460284

Safety of [ 167611-99-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 167611-99-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 167611-99-6 ]

[ 167611-99-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 89466-16-0 ]
  • [ 167611-99-6 ]
  • (1R,2S,5S)-tert-butyl 2-(6-bromo-3-methylpyridin-2-ylcarbamoyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
43% With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 90℃;Inert atmosphere; To a solution of (1R,2S,5S)-3-(tert-butoxycarbonyl)-3-azabicyclo[3.1.0]hexane-2-carboxylic acid (0.19 g, 0.84 mmol) in 1,2-dichloroethane was added ethyl 2-ethoxyquinoline-1(2H)? carboxylate (0.35 g, 1.40 mmol), DIPEA (0.36 g, 2.8 mmol) and <strong>[89466-16-0]6-bromo-3-methylpyridin-2-amine</strong> (80 mg, 0.46 mmol). The reaction was stirred at 90° C. under N2atmosphere overnight. The mixture was concentrated and the residue was purified by column chromatography on silica gel eluted with PE/EtOAc (100:1 to 30:1) to give the desired product (0.12 g, 43.0percent yield); LC/MS (ESI) m/z: 396 [M+H]+
 

Historical Records

Technical Information

Categories