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Chemical Structure| 1634-34-0 Chemical Structure| 1634-34-0

Structure of 1634-34-0

Chemical Structure| 1634-34-0

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Product Details of [ 1634-34-0 ]

CAS No. :1634-34-0
Formula : C9H10O3
M.W : 166.17
SMILES Code : CC(=O)C1=C(O)C=C(C)C=C1O
MDL No. :MFCD06656138
Boiling Point : No data available
InChI Key :CUYUORWXJSURNV-UHFFFAOYSA-N
Pubchem ID :10419531

Safety of [ 1634-34-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1634-34-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1634-34-0 ]

[ 1634-34-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1634-34-0 ]
  • [ 17773-10-3 ]
  • [ 2260-50-6 ]
YieldReaction ConditionsOperation in experiment
93% at 65℃; for 2.0h; Add 3 mol of 3,5-dihydroxy-4-acetyltoluene and 5 mol of iodocholine to the reaction vessel to control the stirring speed.130rpm, raise the temperature to 65 ° C, maintain the temperature and continue to stir until completely dissolved, let stand for 120min, reduce the solution temperatureThe crystal was precipitated to 15 ° C, filtered, and the crystal was washed with a cyclohexane solution having a mass fraction of 85percent, and the mass fraction was 90percent.The toluene solution was washed, and the anhydrous potassium carbonate dehydrating agent was dehydrated to obtain 761.67 g of the finished iodoacetylcholine, and the yield was 93percent
 

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Technical Information

• Acidity of Phenols • Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Bucherer-Bergs Reaction • Chan-Lam Coupling Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Electrophilic Substitution of the Phenol Aromatic Ring • Etherification Reaction of Phenolic Hydroxyl Group • Fischer Indole Synthesis • Friedel-Crafts Reaction • Grignard Reaction • Halogenation of Phenols • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Hydrogenolysis of Benzyl Ether • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Oxidation of Phenols • Passerini Reaction • Paternò-Büchi Reaction • Pechmann Coumarin Synthesis • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Alkylbenzene • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reformatsky Reaction • Reimer-Tiemann Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Tebbe Olefination • Ugi Reaction • Vilsmeier-Haack Reaction • Wittig Reaction • Wolff-Kishner Reduction

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