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Chemical Structure| 16303-60-9 Chemical Structure| 16303-60-9

Structure of 16303-60-9

Chemical Structure| 16303-60-9

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Product Details of [ 16303-60-9 ]

CAS No. :16303-60-9
Formula : C9H6O3
M.W : 162.14
SMILES Code : O=CC1=CC=C(C2=CC=CO2)O1
MDL No. :MFCD06802508
InChI Key :FAGYPMBOOVLXAO-UHFFFAOYSA-N
Pubchem ID :11469241

Safety of [ 16303-60-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501

Application In Synthesis of [ 16303-60-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 16303-60-9 ]

[ 16303-60-9 ] Synthesis Path-Downstream   1~33

  • 1
  • [ 5905-00-0 ]
  • [ 16303-60-9 ]
  • 2
  • [ 16303-60-9 ]
  • [ 51433-48-8 ]
  • [2,2']bifuryl-5-carbaldehyde semicarbazone [ No CAS ]
  • 3
  • [ 16303-60-9 ]
  • [2,2']bifuryl-5-carboxylic acid [ No CAS ]
  • 4
  • [ 7647-01-0 ]
  • [ 5905-00-0 ]
  • [ 60-29-7 ]
  • [ 74-90-8 ]
  • [ 16303-60-9 ]
  • 5
  • [ 584-12-3 ]
  • [ 27329-70-0 ]
  • [ 16303-60-9 ]
  • 6
  • [ 16303-60-9 ]
  • [ 79-40-3 ]
  • 2,5-bis-[2,2']bifuranyl-5-yl-thiazolo[5,4-<i>d</i>]thiazole [ No CAS ]
  • 7
  • [ 1899-24-7 ]
  • [ 118486-94-5 ]
  • [ 16303-60-9 ]
  • 8
  • [ 16303-60-9 ]
  • [2,2']bifuranyl-5-carbaldehyde oxime [ No CAS ]
  • 9
  • [ 16303-60-9 ]
  • [ 1020847-47-5 ]
  • 10
  • [ 16303-60-9 ]
  • [ 1020847-50-0 ]
  • 11
  • [ 16303-60-9 ]
  • [ 915979-04-3 ]
  • 12
  • [ 16303-60-9 ]
  • bis-nitrile 5,5’-bis(5-cyano-2-furanyl)-2,2’-bifuran [ No CAS ]
  • 13
  • [ 13529-27-6 ]
  • [ 16303-60-9 ]
  • 14
  • [ 615-09-8 ]
  • [ 16303-60-9 ]
  • 15
  • [ 5905-06-6 ]
  • [ 16303-60-9 ]
  • 16
  • [ 16303-60-9 ]
  • [ 141580-08-7 ]
YieldReaction ConditionsOperation in experiment
Example 107 Preparation of N-hydroxy-N-[4-(5-{fur-2-yl}-2-furyl)-3-butyn-2-yl]urea The title compound was prepared according to the procedure of Example 106 using 5-(fur-2-yl)furfural instead of 5-phenyfurfural. m.p.: 154.5-156 C. (dec). 1 H NMR (300 MHz, DMSO-d6) δ TMS: 1.38 (d, J=7 Hz, 3H), 5.18 (q, J=7 Hz, 1H), 6.59 (bs, 2H), 6.62 (m, 1H), 6.72 (d, J=4 Hz, 1H), 6.80 (d, J=4 Hz, 1H), 6.85 (d, J=3Hz, 1H), 7.77 (m, 1H), 9.42 (s, 1H). MS (DCI-NH3) m/e, 278 (M+NH4)+, 261 (M+1)+, 185. Anal. Calcd. for C13 H12 N2 O4: C, 60.00; H, 4.65; N, 10.76. Found: C, 59.86; H, 4.50; N, 10.59.
  • 17
  • [ 166328-14-9 ]
  • [ 21508-19-0 ]
  • [ 16303-60-9 ]
  • 18
  • [ 1899-24-7 ]
  • [ 13331-23-2 ]
  • [ 16303-60-9 ]
YieldReaction ConditionsOperation in experiment
77% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; at 70℃;Inert atmosphere; Sealed tube; General procedure: A bromo-aldehyde (1 mmol), boronic acid (1.1e1.3 mmol), tetrakis(triphenylphosphine)palladium (0.05 mmol), potassium carbonate(3 mmol), water (3 ml), ethanol (4 ml) and toluene (4 ml)were added to a round-bottomed flask. The reaction mixture wasflushed with argon, sealed under septa and heated at 70 C overnight.After cooling to room temperature, water (50 ml) was added,and product was extracted with ethyl acetate (3 x 50 ml). Combinedextracts were washed with brine, dried with anhydrousmagnesium sulfate and evaporated under reduced pressure. Theproduct was purified by column chromatography on silica withchloroform or a mixture of methanol and chloroform (1:9).
  • 20
  • [ 16303-60-9 ]
  • [ 1415721-02-6 ]
  • 21
  • [ 16303-60-9 ]
  • [ 1415721-05-9 ]
  • 22
  • [ 16303-60-9 ]
  • [ 1415720-87-4 ]
  • 23
  • [ 16303-60-9 ]
  • 5,5''-dihydroxymethyl-2,2',5',2''-terfuran [ No CAS ]
  • 24
  • [ 16303-60-9 ]
  • [ 1415720-97-6 ]
  • 25
  • [ 16303-60-9 ]
  • 2-(furan-2-yl)furo[3,2-c]pyridin-4(5H)-one [ No CAS ]
  • 26
  • [ 16303-60-9 ]
  • (E)-3-([2,2'-bifuran]-5-yl)acryloyl azide [ No CAS ]
  • 27
  • [ 16303-60-9 ]
  • [ 141-82-2 ]
  • (E)-3-([2,2'-bifuran]-5-yl)acrylic acid [ No CAS ]
  • 28
  • [ 61-54-1 ]
  • [ 16303-60-9 ]
  • ([2,2'-bifuran]-5-yl}methyl)[2-(1H-indol-3-yl)ethyl]amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
42% General procedure: Tryptamine (0.0015 mol) and aldehyde (0.001 mol) were dissolvedin MeOH (3 ml) together with a few pellets of molecularsieve3A. The reaction mixture was stirred overnight at roomtemperature, followed by the addition of NaBH4 (0.002 mol) andstirring of the reaction for 1 h. Water (100 ml) was added, andproductwas extracted with ethyl acetate (3 50 ml). The combinedextracts werewashed with brine, dried over anhydrous magnesiumsulfate and evaporated under reduced pressure. The product waspurified by column chromatography on silica with a mixture ofmethanol and chloroform (1:9).
  • 29
  • [ 16303-60-9 ]
  • [ 2450-71-7 ]
  • C12H9NO2 [ No CAS ]
  • 30
  • [ 16303-60-9 ]
  • N-([2,2′-bifuran]-5-ylmethyl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide [ No CAS ]
  • 31
  • [ 16303-60-9 ]
  • N-([2,2′-bifuran]-5-ylmethyl)-4-methyl-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide [ No CAS ]
  • 32
  • [ 16303-60-9 ]
  • (E)-5-(3-(furan-2-yl)-3-oxoprop-1-en-1-yl)-4-phenyl-1-tosyl-1,6-dihydropyridin-3(2H)-one [ No CAS ]
  • 33
  • [ 16303-60-9 ]
  • [ 769-42-6 ]
  • 5-([2,2'-bifuran]-5-ylmethylene)-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione [ No CAS ]
 

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[ 16303-60-9 ]

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