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Chemical Structure| 16156-56-2 Chemical Structure| 16156-56-2

Structure of 16156-56-2

Chemical Structure| 16156-56-2

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Product Details of [ 16156-56-2 ]

CAS No. :16156-56-2
Formula : C7H14O3S
M.W : 178.25
SMILES Code : CS(=O)(OC1CCCCC1)=O
MDL No. :MFCD26961237
InChI Key :KOGOBKOHQTZGIS-UHFFFAOYSA-N
Pubchem ID :85308

Safety of [ 16156-56-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 16156-56-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 16156-56-2 ]

[ 16156-56-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 16156-56-2 ]
  • [ 1175275-00-9 ]
  • 2
  • [ 16156-56-2 ]
  • [ 35344-95-7 ]
  • 1-cyclohexylpyrazole-4-carbaldehyde [ No CAS ]
YieldReaction ConditionsOperation in experiment
53.91% With caesium carbonate; In N,N-dimethyl-formamide; for 16h;Heating; To a stirred solution of 1H- <strong>[35344-95-7]pyrazole-4-carbaldehyde</strong> 13-4 (220 mg, 2.29 mmol) in DMF (5 mL) was added cesium carbonate (1.86 g, 5 72 mmol) and cyclohexyl methanesulfonate 13-3 (489.74 mg, 2.75 mmol). The reaction mixture was heated at 60C for 16 hours. The reaction mixture was quenched with cold water and extracted with ethyl acetate. The organic layer was washed with a saturated aqueous solution of NaHCCb, dried over NaiSCh and concentrated under reduced pressure to afford crude which was purified by column chromatography to afford l-cyclohexyl<strong>[35344-95-7]pyrazole-4-carbaldehyde</strong> 13-5 (220 mg, 1.23 mmol, 53.91 % yield) as gummy liquid. LC MS: ES+ 179.
 

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