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Chemical Structure| 1595-01-3 Chemical Structure| 1595-01-3

Structure of 1595-01-3

Chemical Structure| 1595-01-3

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Product Details of [ 1595-01-3 ]

CAS No. :1595-01-3
Formula : C13H20
M.W : 176.30
SMILES Code : CC1=CC=C(CCCCCC)C=C1

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Application In Synthesis of [ 1595-01-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1595-01-3 ]

[ 1595-01-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 158136-46-0 ]
  • [ 1595-01-3 ]
  • [ 2150-46-1 ]
  • 5-[[6-([1,1'-Biphenyl]-4-yloxy)hexyl]oxy]-2-hydroxybenzoic acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
56% With potassium carbonate; In water; N,N-dimethyl-formamide; acetone; EXAMPLE 101 5-[[6-([1,1'-Biphenyl]-4-yloxy)hexyl]oxy]-2-hydroxybenzoic acid methyl ester A mixture of 1.0 g (6 mmol) of 2,5-dihydroxybenzoic acid methyl ester, 2.0 g (6 mmol) of 6-([1,1'-biphenyl]-4-yloxy)hexyl bromide and 1.24 g (9 mmol) of potassium carbonate in 50 ml of acetone and 5 ml of DMF was stirred at reflux for 27 hours. The solvents were removed at reduced pressure, water was added to the residue and the product was extracted with ethyl acetate. The dried extract was concentrated to a solid which was purified by chromatography on 40 g of silica gel using 50% toluene-hexane to give 1.4 g (56% yield, mp 91-92) of 5-[[6-([1,1'-biphenyl]4-yloxy)hexyl]oxy]-2-hydroxybenzoic acid methyl ester. The structure was confirmed by nmr and mass spectra.
  • 2
  • [ 74-85-1 ]
  • [ 108-88-3 ]
  • [ 611-14-3 ]
  • [ 622-96-8 ]
  • [ 1595-05-7 ]
  • [ 1595-11-5 ]
  • [ 1595-01-3 ]
  • [ 1595-10-4 ]
 

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