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Chemical Structure| 152192-96-6 Chemical Structure| 152192-96-6

Structure of 152192-96-6

Chemical Structure| 152192-96-6

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Product Details of [ 152192-96-6 ]

CAS No. :152192-96-6
Formula : C10H21NO3
M.W : 203.28
SMILES Code : O=C(OC(C)(C)C)N(CCO)CCC
MDL No. :MFCD06658367

Safety of [ 152192-96-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 152192-96-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 152192-96-6 ]

[ 152192-96-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 22280-60-0 ]
  • [ 152192-96-6 ]
  • [ 954369-02-9 ]
YieldReaction ConditionsOperation in experiment
70.2% With lithium hydride; In toluene; at 90℃; for 4h; u. r2-(5-Amino-6-methyl-pyridin-2-yloxy)-ethyll-propyl-carbamic acid ferf-butyl esteru.1 [2-(6-Methyl-5-nitro-pyridin-2-yloxy)-ethyl]-propyl-carbamic acid te/t-butyl esterA mixture of <strong>[22280-60-0]6-chloro-2-methyl-3-nitro-pyridine</strong> (1 g, 5.79 mmol), (2-hydroxy- ethyl)-propyl-carbamic acid te/t-butyl ester (1.18 g, 5.79 mmol) and lithium hydride (0.05 g, 6.37 mmol) in toluene (5 ml) was stirred at 900C for 4 h. After evaporation of the solvent under reduced pressure the residue was <n="131"/>purified by silica gel chromatography with heptane/ethyl acetate (10:0; 8:2; 0:10) as eluent to provide 1.38 g (70.2percent) of the product.MS (ESI) m/z: 284.15 [M+H(-[terf-butyl])]+
  • 2
  • [ 22280-60-0 ]
  • [ 152192-96-6 ]
  • [ 954369-03-0 ]
 

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