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Chemical Structure| 15126-06-4 Chemical Structure| 15126-06-4

Structure of 15126-06-4

Chemical Structure| 15126-06-4

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Product Details of [ 15126-06-4 ]

CAS No. :15126-06-4
Formula : C8H7IO3
M.W : 278.04
SMILES Code : O=C(OC)C1=CC=C(O)C(I)=C1
MDL No. :MFCD05664378
InChI Key :PXNOLLHARLSLHY-UHFFFAOYSA-N
Pubchem ID :11346465

Safety of [ 15126-06-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H318
Precautionary Statements:P264-P270-P280-P301+P312-P305+P351+P338-P310-P330-P501

Application In Synthesis of [ 15126-06-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15126-06-4 ]

[ 15126-06-4 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 32294-60-3 ]
  • [ 3337-66-4 ]
  • [ 15126-06-4 ]
  • 4-Hydroxy-3-phenyltellanyl-benzoic acid methyl ester [ No CAS ]
  • 4-Hydroxy-3-iodo-5-phenyltellanyl-benzoic acid methyl ester [ No CAS ]
  • 4-Hydroxy-3,5-bis-phenyltellanyl-benzoic acid methyl ester [ No CAS ]
  • 2
  • [ 3337-66-4 ]
  • [ 15126-06-4 ]
  • 3
  • [ 99-76-3 ]
  • [ 3337-66-4 ]
  • [ 15126-06-4 ]
  • 4
  • [ 2914-69-4 ]
  • [ 15126-06-4 ]
  • [ 1393671-30-1 ]
  • 5
  • [ 23152-99-0 ]
  • [ 15126-06-4 ]
  • N-hydroxy-2-[4-(1-methylethyl)phenyl]-1-benzofuran-5-carboxamide [ No CAS ]
  • 6
  • [ 23152-99-0 ]
  • [ 15126-06-4 ]
  • C19H18O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 100℃; for 0.5h;Inert atmosphere; Microwave irradiation; Pd(PPh3)2Cl2 (8.6 mg, 0.012 mmol) was added to a nitrogen flushed mixture of methyl 4- hydroxy-3-iodobenzoate (34 mg, 0.122 mmol), 4-isopropylphenylacetylene (26.4 mg, 0.183 mmol), Cul (4.6 mg, 0.024 mmol) and Et3N ( 24.7 mg, 0.245 mmol) in THF (2 ml). The mixture was heated at 100 C for 30 min in a microwave reactor. Solvent was evaporated and residue purified by flash chromatography using 5%-10% EtOAc in heptanes. Yield: 14.4 mg (40%); yellow solid. MS (ESI+) m/z 295 [M+H]+. HPLC purity: 80%.
  • 7
  • [ 381-98-6 ]
  • [ 15126-06-4 ]
  • methyl 2-oxo-3-(trifluoromethyl)-2H-chromenyl-6-carboxylate [ No CAS ]
 

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