Home Cart Sign in  
Chemical Structure| 150879-48-4 Chemical Structure| 150879-48-4

Structure of 150879-48-4

Chemical Structure| 150879-48-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 150879-48-4 ]

CAS No. :150879-48-4
Formula : C9H11ClN2O2
M.W : 214.65
SMILES Code : O=C(N(OC)C)C1=CC(Cl)=CC=C1N
MDL No. :MFCD12095383

Safety of [ 150879-48-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 150879-48-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150879-48-4 ]

[ 150879-48-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 150879-48-4 ]
  • [ 141-78-6 ]
  • [ 171663-13-1 ]
  • [ 214956-91-9 ]
YieldReaction ConditionsOperation in experiment
With n-butyllithium; In tetrahydrofuran; hexane; water; (1) A solution of N-methyl-N-methyloxy-2-amino-5-chlorobenzamide (24.8 g) and <strong>[171663-13-1]N-tert-butoxycarbonyl-3-bromobenzylamine</strong> (22.0 g) in tetrahydrofuran (300 ml) was cooled to -78 C. To the solution was gradually added dropwise a hexane solution (1.6 mol./L)(240 ml) of n-butyl lithium. To the mixture were then added water (300 ml) and acetic acid ethyl ester (300 ml). The organic layer was washed with water, which was dried over anhydrous MgSO4, then the solvent was distilled off. To the residual oily compound was added hexane (400 ml) to cause crystallization. The crystalline product was collected by filtration to give 2-amino-3'-tert-butoxycarbonylaminomethyl-5-chlorobenzophenone (12.5 g) as pale yellow crystals.
 

Historical Records

Technical Information

Categories