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Chemical Structure| 143-27-1 Chemical Structure| 143-27-1

Structure of Cetylamine
CAS No.: 143-27-1

Chemical Structure| 143-27-1

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Product Details of [ 143-27-1 ]

CAS No. :143-27-1
Formula : C16H35N
M.W : 241.46
SMILES Code : NCCCCCCCCCCCCCCCC
MDL No. :MFCD00008158
InChI Key :FJLUATLTXUNBOT-UHFFFAOYSA-N
Pubchem ID :8926

Safety of [ 143-27-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H410
Precautionary Statements:P264-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P403+P233-P501
Class:8
UN#:3259
Packing Group:

Application In Synthesis of [ 143-27-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 143-27-1 ]

[ 143-27-1 ] Synthesis Path-Downstream   1~9

  • 1
  • [ 143-27-1 ]
  • [ 57-92-1 ]
  • [ 56222-72-1 ]
  • 2
  • [ 629-54-9 ]
  • [ 143-27-1 ]
YieldReaction ConditionsOperation in experiment
With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; The crude product was suspended in THF (50 mL) and treated withlithium aluminum hydride (1.1 g, added slowly). The reaction mixture was stirred for an hour. Excess methanol was added slowly, followed by water (2mL). Dichloromethane(200 mL) was added and the mixture filtered. The solvent was removed from the filtrate, yielded crude hexadecylamine (7 g)
  • 3
  • [ 143-27-1 ]
  • [ 97-08-5 ]
  • [ 118938-20-8 ]
YieldReaction ConditionsOperation in experiment
88% With triethylamine; In methanol; dichloromethane; Synthesis Example 2-3 Synthesis of 4-chloro-3-nitro-N-hexadecylbenzenesulfonamide: To 4-chloro-3-nitrobenzenesulfonyl chloride obtained in the above step was added 1 liter of dichloromethane and the mixture was cooled to 0 C. To the solution formed was added dropwise a mixture of 600 g of hexadecylamine, 251 ml of triethylamine, and 780 ml of dichloromethane at 20 C. to 30 C. After performing reaction for 2 hours at room temperature, the dichloromethane was distilled off from the reaction mixture under reduced pressure and the residue thus formed was dissolved in 3 liters of methanol under heating. The mixture was gradually cooled to deposit crystals at room temperature, 3 liters of methanol was added to the system while ice-cooling to further deposit crystals, and the crystals formed were recovered by filtration and dried to provide 1020 g of the above-described compound with a yield of 88%. The melting point thereof was 91 C. to 93 C.
  • 4
  • [ 143-27-1 ]
  • [ 6914-79-0 ]
  • [ 1266666-37-8 ]
  • 5
  • [ 143-27-1 ]
  • [ 6914-79-0 ]
  • [ 1266665-36-4 ]
  • 6
  • [ 143-27-1 ]
  • [ 25834-16-6 ]
  • [ 1613460-24-4 ]
  • 7
  • [ 143-27-1 ]
  • [ 1124-13-6 ]
  • C38H74N2O2 [ No CAS ]
  • 8
  • [ 143-27-1 ]
  • [ 610-09-3 ]
  • C40H78N2O2 [ No CAS ]
  • 9
  • [ 143-27-1 ]
  • [ 629-54-9 ]
 

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