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Chemical Structure| 142355-81-5 Chemical Structure| 142355-81-5

Structure of 142355-81-5

Chemical Structure| 142355-81-5

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Product Details of [ 142355-81-5 ]

CAS No. :142355-81-5
Formula : C14H26BrNO2
M.W : 320.27
SMILES Code : BrCCCCC1CCN(C(OC(C)(C)C)=O)CC1
MDL No. :MFCD07369864

Safety of [ 142355-81-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 142355-81-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 142355-81-5 ]

[ 142355-81-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 64205-12-5 ]
  • [ 142355-81-5 ]
  • 4-{4-[4-((R)-2-Benzyloxycarbonylamino-2-carboxy-ethyl)-phenoxy]-butyl}-piperidine-1-carboxylic acid tert-butyl ester [ No CAS ]
  • 2
  • [ 142355-83-7 ]
  • [ 142355-81-5 ]
YieldReaction ConditionsOperation in experiment
With carbon tetrabromide; triphenylphosphine; In acetonitrile; at 20℃; for 1h; Tert-butyl 4- (4-hydroxybutyl) piperidine-1-carboxylate (3 g, 11.67 mmol) was added to a round bottom flask, and the reaction product was dissolved in acetonitrile (40 mL). Then, triphenylphosphine (6 g) and carbon tetrabromide (9 g) were added. At room temperatureThe mixture was stirred for 1 hour and extracted several times with ethyl acetate. The organic layer was washed with water and saturated sodium chloride solution, dried over sodium sulfate, and then concentrated. The obtained filtrate was purified by chromatography to obtain the desired compound as a colorless liquid.
  • 3
  • [ 7037-49-2 ]
  • [ 142355-81-5 ]
 

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