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Chemical Structure| 13360-63-9 Chemical Structure| 13360-63-9
Chemical Structure| 13360-63-9

N-Ethylbutylamine

CAS No.: 13360-63-9

4.5 *For Research Use Only !

Cat. No.: A228987 Purity: 98%

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Product Details of [ 13360-63-9 ]

CAS No. :13360-63-9
Formula : C6H15N
M.W : 101.19
SMILES Code : CCCCNCC
MDL No. :MFCD00009428

Safety of [ 13360-63-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H302-H314
Precautionary Statements:P210-P280-P305+P351+P338-P310
Class:3(8)
UN#:2733
Packing Group:

Application In Synthesis of [ 13360-63-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13360-63-9 ]

[ 13360-63-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13360-63-9 ]
  • [ 146137-78-2 ]
  • [ 945847-39-2 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In toluene;Heating / reflux; 2-Fluoro-5-trifluoromethyl-benzaldehyde (5.Og) and butyl-ethyl- amine (3.95g) are dissolved in toluene (50ml) and thereto is added potassium carbonate (10.78g) and the mixture is heated under reflux overnight. The reaction solution is cooled to room temperature, and thereto are added water and diethyl ether, and the mixture is separated, and the organic layer is washed with a saturated brine, dried over magnesium sulfate, and concentrated under reduced pressure. The resulting residue is purified by silica gel column chromatography (hexane : ethyl acetate = 19: 1- »4: 1) to give 2~(butyl-ethyl-amino)-5-trifluoromethyl- benzaldehyde (6.54g). MS (m/z): 274 [M+H]+.
 

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