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Chemical Structure| 132622-68-5 Chemical Structure| 132622-68-5

Structure of 132622-68-5

Chemical Structure| 132622-68-5

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Product Details of [ 132622-68-5 ]

CAS No. :132622-68-5
Formula : C10H16N4O4
M.W : 256.26
SMILES Code : O=C([C@H]1N(C(OC(C)(C)C)=O)C[C@H](N=[N+]=[N-])C1)O
MDL No. :MFCD12923197

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Application In Synthesis of [ 132622-68-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 132622-68-5 ]

[ 132622-68-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 132622-68-5 ]
  • [ 132622-69-6 ]
  • 2
  • trans azido acid [ No CAS ]
  • [ 132622-68-5 ]
  • [ 132622-69-6 ]
  • [ 132622-66-3 ]
YieldReaction ConditionsOperation in experiment
67% EXAMPLE 8 STR12 (4R)-1-(tert-Butoxycarbonyl)-4-amino-L-proline (9). The trans azido acid 8b (3.0 g., 11.7 mmol) was hydrogenated as for the synthesis of 6, to give 1.8 g (67% yield) after crystlalization from ethanol, m.p.=228-229 C. (decomp.). 1 H NMR (CDCl3) δ1.42/1.47 (2s, 9H), 2.29 (m, 1H), 2.45 (m, 1H), 3.58 (m, 1H), 3.80 (m, 1H), 3.99 (m, 1H), 4.24 (m, 1H). Anal. (C10 H18 N2 O4.0.5H2 O) C, H, N.
 

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