Home Cart Sign in  
Chemical Structure| 1310796-19-0 Chemical Structure| 1310796-19-0

Structure of 1310796-19-0

Chemical Structure| 1310796-19-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1310796-19-0 ]

CAS No. :1310796-19-0
Formula : C13H22N2O3
M.W : 254.33
SMILES Code : O=C1/C(CN(C(OC(C)(C)C)=O)CC1)=C\N(C)C
MDL No. :MFCD08443986

Safety of [ 1310796-19-0 ]

Application In Synthesis of [ 1310796-19-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 1310796-19-0 ]
  • Downstream synthetic route of [ 1310796-19-0 ]

[ 1310796-19-0 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 1310796-19-0 ]
  • [ 230301-11-8 ]
YieldReaction ConditionsOperation in experiment
95% With hydrazine hydrate In ethanol at 20℃; for 12 h; To a solution of (Z)-tert-butyl 3-((dimethylamino)methylene)-4-oxopiperidine-i- carboxylate (8.8 g, 34.6 mmol) in EtOH (50 mL) was added N2H4/H20 (200 mL) at 20 °C. The mixture was stuffed at 20 °C for 12 h. After that, the reaction mixture was concentrated in vacuum. The residue mixture was purified with column separation to afford desired product (7 g, Yield 95 percent). LCMS (mlz): 224.2 [M+H] .
References: [1] Patent: WO2015/200677, 2015, A2, . Location in patent: Paragraph 00806; 00807.
 

Historical Records