Home Cart Sign in  
Chemical Structure| 13096-62-3 Chemical Structure| 13096-62-3

Structure of 13096-62-3

Chemical Structure| 13096-62-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 13096-62-3 ]

CAS No. :13096-62-3
Formula : C34H34O6
M.W : 538.63
SMILES Code : O=C(O5)[C@@H]([C@H]([C@@H]([C@H]5COCC4=CC=CC=C4)OCC3=CC=CC=C3)OCC2=CC=CC=C2)OCC1=CC=CC=C1
MDL No. :MFCD08703228
InChI Key :BUBVLQDEIIUIQG-NXVJRICRSA-N
Pubchem ID :10907626

Safety of [ 13096-62-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H413
Precautionary Statements:P264-P270-P273-P301+P312-P330

Application In Synthesis of [ 13096-62-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13096-62-3 ]

[ 13096-62-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 13096-62-3 ]
  • [ 149-32-6 ]
  • 1,2:3,4-di-O-(2,3,4,6-tetra-O-benzyl-D-glucopyranosylidene)erythritol [ No CAS ]
  • 2
  • [ 13096-62-3 ]
  • [ 57310-39-1 ]
  • C41H41ClO6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
The title compound was prepared from 39 in the same manner as described for 33 (63% yield over two steps, a colorless oil).1H NMR (CDCl3) delta: 2.31 (3H, s), 3.58-3.90 (6H, m), 3.96 (1H, d, J = 10.6 Hz), 4.38 (1H, d, J = 10.4 Hz), 4.50-4.68 (3H, m), 4.78-4.98 (4H, m), 6.91-7.08 (3H, m), 7.12-7.38 (20H, m). MS (FAB) m/z: 649 (M++H), calcd for C41H41ClO5: 648.
  • 3
  • [ 13096-62-3 ]
  • [ 1030825-20-7 ]
  • (3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)-2-(3-((5-(4-fluorophenyl)thiophen-2-yl)methyl)-4-methylphenyl)tetrahydro-2H-pyran-2-ol [ No CAS ]
YieldReaction ConditionsOperation in experiment
99% Under an argon atmosphere, 300 mL of dehydrated tetrahydrofuran and 90.4 g (250 mmol)2- (2-methyl-5-bromobenzyl) -5- (4-fluorophenyl) thiophene was added to 1000 mLIn a three-neck flask,The temperature of the mixed system was controlled at -78 ° C with an acetone / dry ice bath,To the three-necked flask, 100 mL (2.5 mol / L, 250 mmol, 1 eq)Butyl lithium,The temperature of the reaction system during the dropwise addition was controlled at -78 ° C,After completion of the dropwise addition,And allowed to stand at -78 ° C for 1 hour.Was added dropwise to the reaction system2,3,4,6-tetra-O-benzyl-D-gluconolactone in tetrahydrofuran(2,3,4,6-tetra-O-benzyl-D-gluconolactone, 135.6 g,Tetrahydrofuran (150 mL)While stirring while stirring,After the dropwise addition, the dry ice / acetone bath was removed,The temperature of the reaction system was gradually returned to room temperature, and the reaction was allowed to proceed for 3 hoursAfter the reaction was stopped,The reaction was quenched with saturated NaHCO3 solution under ice-cooling,After quenching, the reaction product solution was extracted with ethyl acetate,The organic phases are combined,Dried over magnesium sulfate and concentrated under reduced pressure,210.1 g of a yellow thick liquid was obtained. The yellow thick liquid was detected and collectedThe results indicated that the yellow thick liquid had the structure of the formula (II-I), the purity was 87.7percentThe yield was 99percent
 

Historical Records