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Chemical Structure| 1301161-41-0 Chemical Structure| 1301161-41-0

Structure of 1301161-41-0

Chemical Structure| 1301161-41-0

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Product Details of [ 1301161-41-0 ]

CAS No. :1301161-41-0
Formula : C36H23BrN2
M.W : 563.49
SMILES Code : BrC1=CC2=C(C=C1)N(C3=CC=C(C4=CC=C(N5C6=C(C7=C5C=CC=C7)C=CC=C6)C=C4)C=C3)C8=C2C=CC=C8

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Application In Synthesis of [ 1301161-41-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1301161-41-0 ]

[ 1301161-41-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 867044-33-5 ]
  • [ 1301161-41-0 ]
  • 3-(2-phenyl-N-4-phenylbenzimidazolyl)-N,N'-dicarbazolyl-4,4'-biphenyl [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; toluene; for 24h;Inert atmosphere; Reflux; 3-bromo-N, N'-dicarbazolyl-4,4'-biphenyl (1.0 mmol), 2-phenyl-N-4-phenyl-benzo (0.1 mmol), tetrakis (triphenylphosphine)palladium (Pd (PPh 3) 4) (0.05 mmol), potassium carbonate (K 2 CO 3) (2M, 10 ml), toluene (50 ml), ethanol (20 ml), and the aircontained in the solution was driven off by the addition of nitrogen. The resulting solution was heated under reflux in a nitrogenatmosphere for 24 hours. The reaction solution was cooled to room temperature, extracted three times with dichloromethane,washed three times with water, Dried over anhydrous magnesium sulfate, filtered and evaporated to dryness under reducedpressure to give the crude product which was sublimed directly with a sublimation machine to give a white solid product in 75%yield.
 

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