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Chemical Structure| 1294411-24-7 Chemical Structure| 1294411-24-7

Structure of 1294411-24-7

Chemical Structure| 1294411-24-7

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Product Details of [ 1294411-24-7 ]

CAS No. :1294411-24-7
Formula : C37H25N3
M.W : 511.62
SMILES Code : N1(C2=CC=CC=C2)C3=C(C4=C1C=CC=C4)C=C(C5=CC=C(C6=NC7=CC=CC=C7N6C8=CC=CC=C8)C=C5)C=C3
MDL No. :MFCD28291913

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Application In Synthesis of [ 1294411-24-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1294411-24-7 ]

[ 1294411-24-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1153-85-1 ]
  • [ 952514-79-3 ]
  • [ 1294411-24-7 ]
YieldReaction ConditionsOperation in experiment
80% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; for 6h;Inert atmosphere; Reflux; 3-BrPCz (6.44g, 0.02mol) was added to a three-necked flask, BnImBA (6.91g, 0.022mol), aqueous potassium carbonate (38.3g, 0.06mol), 100ml of toluene, 50ml of ethanol; under nitrogen with stirring was added Pd (PPh3)4(0.23g, 0.2mmol), after the replacement with nitrogen, the reaction was refluxed for 6 hours; after completion of the reaction, was cooled to room temperature, the layers were separated and the organic phase was washed with saturated aqueous sodium chloride solution until neutral, dried over anhydrous sodium sulfate and filtered to give a brown liquid; The solvent was removed by rotary evaporation, silica gel column, eluent VPetroleum ether: VEthyl acetate= 1: 1 was purified to obtain the white solid in 80% yield.
 

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