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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 1289556-30-4 Chemical Structure| 1289556-30-4

Structure of 1289556-30-4

Chemical Structure| 1289556-30-4

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Product Details of [ 1289556-30-4 ]

CAS No. :1289556-30-4
Formula : C21H30S3Sn3
M.W : 734.79
SMILES Code : C[Sn](C)(C)C1=CC(C2=C(C=C([Sn](C)(C)C)S2)C3=C4C=C(S3)[Sn](C)(C)C)=C4S1
MDL No. :N/A

Safety of [ 1289556-30-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H300+H310+H330-H410
Precautionary Statements:P260-P262-P264-P270-P271-P273-P280-P284-P301+P310+P330-P302+P352+P310-P304+P340+P310-P361+P364-P391-P403+P233-P405-P501
Class:6.1
UN#:3146
Packing Group:

Application In Synthesis of [ 1289556-30-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1289556-30-4 ]

[ 1289556-30-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 29150-63-8 ]
  • [ 1066-45-1 ]
  • [ 1289556-30-4 ]
YieldReaction ConditionsOperation in experiment
94% Under nitrogen, a 100 mL Schlenk flask was charged with compound 3 (1.14 g, 4.6 mmol) and anhydrous tetrahydrofuran(50 mL) was added and the solution was cooled to -78 C. A solution of n-butyllithium in hexane (11.6 mL, 2.4M) was slowly added dropwise to the solution, After stirring, the reaction was continued for 1 hour at -78 C. Then, trimethyltin chloride (12 mL, 1.0 M) was added. The reaction was continued for 1 hour while maintaining the temperature and the system was stirred overnight at room temperature. The organic phase was extracted with dichloromethane, and the combined organic phases were washed successively with saturated brine and water, dried over anhydrous sodium sulfate, filtered, and the organic solvent was removed by rotary evaporation, and recrystallized from ethanol to obtain white solid 4 (3.18g, 94 %).
 

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