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Chemical Structure| 1283120-11-5 Chemical Structure| 1283120-11-5

Structure of 1283120-11-5

Chemical Structure| 1283120-11-5

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Product Details of [ 1283120-11-5 ]

CAS No. :1283120-11-5
Formula : C7H11N3O2
M.W : 169.18
SMILES Code : O=C(C1=CN(C)N=C1)N(OC)C
MDL No. :MFCD18840273

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Application In Synthesis of [ 1283120-11-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1283120-11-5 ]

[ 1283120-11-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1283120-11-5 ]
  • [ 75-16-1 ]
  • [ 37687-18-6 ]
YieldReaction ConditionsOperation in experiment
8 mg In tetrahydrofuran; at -78 - 20℃; for 14h; Method 31 Synthesis of 2-bromo-1-(6-methyl-3-pyridyl)ethanone (Intermediate 45) To a solution of R-12 (10 g, 79.3 mmol) in MeCN (200 mL) at 0 C. is added N,O-dimethylhydroxylaminehydrochloride (8.5 g, 87.2 mmol), EDCI (18.2 g, 95.2 mmol), 1-hydroxybenzotriazole (3.2 g, 23.8 mmol) followed by triethylamine (20.5 mL, 158 mmol) and stirred at room temperature 15 h. The reaction mixture is partitioned between water and EtOAc. The collected organics are dried with anhydrous Na2SO4, filtered, and concentrated in vacuo to give I-43 (12 g) m/z 170.0 [M+H].
 

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