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Chemical Structure| 127349-56-8 Chemical Structure| 127349-56-8
Chemical Structure| 127349-56-8

1-(Bromomethyl)-2-fluoro-4-nitrobenzene

CAS No.: 127349-56-8

4.5 *For Research Use Only !

Cat. No.: A133794 Purity: 97%

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Product Details of [ 127349-56-8 ]

CAS No. :127349-56-8
Formula : C7H5BrFNO2
M.W : 234.02
SMILES Code : O=[N+](C1=CC=C(CBr)C(F)=C1)[O-]
MDL No. :MFCD10000853
Boiling Point : No data available
InChI Key :TWQCQFRJJOQBRP-UHFFFAOYSA-N
Pubchem ID :21886132

Safety of [ 127349-56-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H335-H314
Precautionary Statements:P260-P264-P270-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P403+P233-P405-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 127349-56-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 127349-56-8 ]

[ 127349-56-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 660432-43-9 ]
  • [ 127349-56-8 ]
YieldReaction ConditionsOperation in experiment
85% With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 23℃; for 2h; Step 2: To a cooled (0 C) and stirred solution of DCM (100 mL) containing <strong>[660432-43-9](2-fluoro-4-nitrophenyl)methanol</strong> (9 g, 52.6 mmol, 1 eq), triphenylphosphine (16.5 g, 63.1 mmol, 1 .2 eq) was added followed by addition of NBS (1 1 .24 g, 63.1 mmol, 1 .2 eq), the mixture was allowed to warm to RT and stirred for 2 h. The DCM was evaporated under reduced pressure and the residue was purified by CC using PE/EtOAc (9:1 ) as eluent to get l -(bromomethyl)-2-fluoro-4-nitrobenzene (10.50 g, 85%; TLC system: PE/EtOAc (7:3), Rf: 0.6).
 

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