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Chemical Structure| 1262866-93-2 Chemical Structure| 1262866-93-2

Structure of 1262866-93-2

Chemical Structure| 1262866-93-2

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Product Details of [ 1262866-93-2 ]

CAS No. :1262866-93-2
Formula : C20H13ClN2
M.W : 316.78
SMILES Code : ClC1=NC(C2=CC=C(C3=CC=CC=C3)C=C2)=C4C=CC=CC4=N1
MDL No. :MFCD28967157
InChI Key :VSMPNDGQPFFGPG-UHFFFAOYSA-N
Pubchem ID :87160724

Safety of [ 1262866-93-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 1262866-93-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1262866-93-2 ]

[ 1262866-93-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1262866-93-2 ]
  • [ 1257220-47-5 ]
  • [ 1373227-56-5 ]
YieldReaction ConditionsOperation in experiment
70% Compound 12-2 (5g, 17.64mmol) and DMF (100mL) were mixed, and NaH (1.1g, 26.46mmol, 60% dispersion in mineral oil) was slowly added to the mixture. The mixture was stirred at room temperature for 30 minutes. After stirring, 4-(biphenyl-4-yl)-2-chloroquinazoline(5.6g, 17.64mmol) was slowly added to the mixture and stirred for 4 hours. After stirring, a solid product was obtained by adding distilled water (300mL) to the reaction mixture and stirring the reaction mixture for 30 minutes. Column separation was conducted on the solid product, yielding Compound 3 (6.9g, 70%). MS/EIMS: 563.69(found), 563.24(calculated)
 

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