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Chemical Structure| 125987-94-2 Chemical Structure| 125987-94-2

Structure of 125987-94-2

Chemical Structure| 125987-94-2

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Product Details of [ 125987-94-2 ]

CAS No. :125987-94-2
Formula : C6H14N2O4S
M.W : 210.25
SMILES Code : O=C(OC(C)(C)C)NS(=O)(NC)=O

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Application In Synthesis of [ 125987-94-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 125987-94-2 ]

[ 125987-94-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 125987-94-2 ]
  • [ 72179-84-1 ]
YieldReaction ConditionsOperation in experiment
General procedure: Trifluoroacetic acid (240mmol) in CH2Cl2 (20mL) was added dropwise to a stirred suspension of N-alkylsulfamoylcarbamate 6 (80mmol) in CH2Cl2 (100mL) at 0C. The solution was stirred overnight and allowed to warm to ambient temperature. The solution was concentrated in vacuo and the residue was taken up in EtOAc (75mL), washed with sat. NaHCO3 solution (2×50mL), dried (Na2SO4) and concentrated to a colourless oil. Compound 7b required no purification. All other species were isolated by column chromatography (5% MeOH/CH2Cl2) as crystalline solids or pale oils with literature properties.14,15
 

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