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Chemical Structure| 122447-72-7 Chemical Structure| 122447-72-7

Structure of 122447-72-7

Chemical Structure| 122447-72-7

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Product Details of [ 122447-72-7 ]

CAS No. :122447-72-7
Formula : C28H17Br
M.W : 433.34
SMILES Code : BrC1=C2C=CC=CC2=C(C3=C4C=CC=CC4=CC5=CC=CC=C35)C6=CC=CC=C16
MDL No. :MFCD20488012
Boiling Point : No data available

Safety of [ 122447-72-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 122447-72-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 122447-72-7 ]

[ 122447-72-7 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 1055-23-8 ]
  • [ 122447-72-7 ]
YieldReaction ConditionsOperation in experiment
37% With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 0 - 20℃; for 5h;Darkness; 9,9?-bianthracene (10 g, 28.2 mmol) was dissolved in DMF (200 mL), protected from light and N-bromosuccinimide (5.5 g, 31 mmol) diluted in DMF (20 ml) was added to the solution at 0 C. The reaction mixture was maintained at 0 C. for 1 hour. The solution was then warmed slowly to room temperature and stirred for 4 h. After the reaction completion, water was added to the mixture to terminate the reaction. The reaction mixture was extracted with ethyl acetate and water, dried with anhydrous magnesium sulfate, the solvent was removed and the residue was purified by column chromatography on silica(hexane-dichloromethane) to give product 4.5 g (37%) as a yellow solid.
 

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