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Chemical Structure| 120359-56-0 Chemical Structure| 120359-56-0

Structure of 120359-56-0

Chemical Structure| 120359-56-0

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Product Details of [ 120359-56-0 ]

CAS No. :120359-56-0
Formula : C8H6Br2
M.W : 261.94
SMILES Code : C=CC1=CC(Br)=CC(Br)=C1

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Application In Synthesis of [ 120359-56-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 120359-56-0 ]

[ 120359-56-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 120359-56-0 ]
  • [ 59785-43-2 ]
YieldReaction ConditionsOperation in experiment
74% With hydrogen;palladium hydroxide on carbon; In tetrahydrofuran; at 20℃; for 5h; Step B 1, 3-Dibromo-5-ethyl-benzene A mixture of 1, 3-dibromo-5-vinyl-benzene (4.55 g, 17.4 mmol) and 20% Pd (OH) 2/C (2.0 g) in THF (60 mL) is purged with N2 and then H2, and the mixture is stirred under a H2 balloon at rt for 5 hours. The mixture is filtered through hyflo, and the solvent is removed in vacuo to afford crude product that is absorbed on silica gel and purified by flash chromatography using 15/1 hexanes/ethyl acetate to afford 3.38 g (74%) of the title compound. Rf = 0.63 (9/1 hexanes/EtOAc).'H NMR (400 MHz, CDCl3).
 

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