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Chemical Structure| 120266-84-4 Chemical Structure| 120266-84-4

Structure of 120266-84-4

Chemical Structure| 120266-84-4

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Product Details of [ 120266-84-4 ]

CAS No. :120266-84-4
Formula : C10H6N2O6
M.W : 250.16
SMILES Code : O=C(C1=C2C=CC=NN2C(C(O)=O)=C1C(O)=O)O
MDL No. :MFCD28405649

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Application In Synthesis of [ 120266-84-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 120266-84-4 ]

[ 120266-84-4 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 120266-84-4 ]
  • [ 118768-13-1 ]
YieldReaction ConditionsOperation in experiment
62% at 100℃; for 4 h; A mixture of compound B-272 (3.0 g, 12 mmol) in 36percent hydrochloric acid (30 mL) was refluxed for 4 hours. On completion, the reaction mixture was cooled to room temperature. The solid was collected by filtration and washed with water to give compound Β· 273 (1.2 g, 62percent yield) as a green solid.
References: [1] Patent: WO2015/66371, 2015, A1, . Location in patent: Paragraph 00542-00543.
[2] Journal of Organic Chemistry, 1956, vol. 21, p. 764.
 

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