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Chemical Structure| 1194601-82-5 Chemical Structure| 1194601-82-5

Structure of 1194601-82-5

Chemical Structure| 1194601-82-5
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Product Details of [ 1194601-82-5 ]

CAS No. :1194601-82-5
Formula : C24H15NO
M.W : 333.38
SMILES Code : N1(C2=CC=C3OC4=CC=CC=C4C3=C2)C5=C(C6=C1C=CC=C6)C=CC=C5

Safety of [ 1194601-82-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 1194601-82-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1194601-82-5 ]

[ 1194601-82-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5408-56-0 ]
  • [ 86-74-8 ]
  • [ 1194601-82-5 ]
YieldReaction ConditionsOperation in experiment
7.9 g <strong>[5408-56-0]2-Iododibenzofuran</strong> (11.0 g, 37.4 mmol) and carbazole (7.2 g, 43.0 mmol) were dissolved in 1,4-dioxane (250 ml) at room temperature under nitrogen. After 30 min, trans-1,2-diaminocyclohexane (2.0ml, 18.7mmol) was added to the solution and the solution was refluxed overnight. After cooling to room temperature, the solution was extracted using methylene chloride. Methylene chloride was removed by evaporation and obtained product was purified by column chromatography on silica gel using toluene/n-hexane (1: 2) as an eluent. A white powder was obtained as a product (7.9g, yield: 63%). (0007) 1H NMR (400MHZ, CDCl3): delta 8.17 (d, 2H, J=3.8Hz), 8.11 (d, 1H, J=1Hz), 7.94 (d, 1H, J=4Hz), 7.78 (d, 1H, J=4Hz), 7.66-7.59 (m, 2H), 7.54-7.50 (m, 1H), 7.41-7.35 (m, 5H), 7.31-7.25 (m, 2H).
 

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