Home Cart Sign in  
Chemical Structure| 1181329-14-5 Chemical Structure| 1181329-14-5

Structure of 1181329-14-5

Chemical Structure| 1181329-14-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1181329-14-5 ]

CAS No. :1181329-14-5
Formula : C13H16BClO3
M.W : 266.53
SMILES Code : O=C(Cl)C1=CC=CC(B2OC(C)(C)C(C)(C)O2)=C1
MDL No. :MFCD20489143

Safety of [ 1181329-14-5 ]

Application In Synthesis of [ 1181329-14-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1181329-14-5 ]

[ 1181329-14-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1181329-14-5 ]
  • [ 19008-43-6 ]
  • [ 1181329-12-3 ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; In n-heptane; dichloromethane; at 20℃; for 13h; A mixture of <strong>[19008-43-6]benzyl 4-aminobenzoate</strong> (4.39 g, 19.3 mmol), 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoyl chloride (4.30 g, 16.1 mmol) and N,N-diisopropylethylamine (7.49 g, 57.9 mmol) in methylene chloride (50 mL) was stirred at ambient temperature for 13 h. After this time, the reaction was concentrated under reduced pressure and purified by chromatography (silica, heptane to 1:3 ethyl acetate/heptane) to afford benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate (3.07 g, 78% pure by mass, 27% yield) as a light yellow sticky foam that was used without further purification.
 

Historical Records

Technical Information

Categories