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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 117428-51-0 Chemical Structure| 117428-51-0

Structure of 117428-51-0

Chemical Structure| 117428-51-0

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Product Details of [ 117428-51-0 ]

CAS No. :117428-51-0
Formula : C12H13ClO3
M.W : 240.68
SMILES Code : O=C(OC)/C(C1=CC=CC=C1CCl)=C/OC
MDL No. :MFCD14635207

Safety of [ 117428-51-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314
Precautionary Statements:P264-P270-P271-P280-P303+P361+P353-P304+P340-P305+P351+P338-P310-P330-P331-P363-P403+P233-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 117428-51-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 117428-51-0 ]

[ 117428-51-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 117428-51-0 ]
  • [ 34486-06-1 ]
  • picoxystrobin [ No CAS ]
  • 2
  • [ 117428-51-0 ]
  • [ 55690-60-3 ]
  • [ 1070975-53-9 ]
YieldReaction ConditionsOperation in experiment
92% 1 mol (197 g) of 6-methoxy-2-indolylbenzothiazole (2) was added to a 1000 ml round bottom flask, while 500 g of DMF and 40 g of sodium hydroxide were added.Stir at 25 C for half an hour, then add 1 mole (240.5 grams) of (E)-2 - (2'-chloromethyl) phenyl-3-methoxy acrylate methyl ester (1), heated to 80 C, The reaction was completed until the disappearance of the starting material, the reaction time was about 5 hours, the reaction was stopped, filtration was carried out, the solvent was removed, and ethanol was recrystallized to obtain 370 g of a product, purity 97%, yield 92%.
 

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