Home Cart Sign in  
Chemical Structure| 1104807-10-4 Chemical Structure| 1104807-10-4

Structure of 1104807-10-4

Chemical Structure| 1104807-10-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1104807-10-4 ]

CAS No. :1104807-10-4
Formula : C5H3ClINO2S
M.W : 303.51
SMILES Code : IC1=CN=C(S(=O)(Cl)=O)C=C1

Safety of [ 1104807-10-4 ]

Application In Synthesis of [ 1104807-10-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1104807-10-4 ]

[ 1104807-10-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 191478-99-6 ]
  • [ 1104807-10-4 ]
  • methyl 2,6-difluoro-4-[(5-iodopyridin-2-yl)sulfonyl]amino}benzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
69% With pyridine; In dichloromethane; at 20℃; for 12.0h; 5-Iodopyridine-2-sulfonyl chloride (5.1 g, 17 mmol) and <strong>[191478-99-6]methyl 4-amino-2,6-difluorobenzoate</strong> (2.5 g, 13 mmol) were dissolved in methylene chloride (25 ml), and pyridine (5.0 ml) was added thereto, followed by stirring at room temperature for 12 hours. The reaction solution was concentrated under reduced pressure. To the obtained residue, 6 N hydrochloric acid (100 ml) was added. The precipitated solid was filtered, and dried under reduced pressure to obtain the title compound (3.0 g, 69%). [0261] 1H NMR (d-DMSO, 400 MHz): delta 11.58 (br, 1H), 9.00 (d, J=2.0 Hz, 1H), 8.54-8.51 (dd, J=8.4, 2.0 Hz, 1H), 7.92 (d, J=8.0 Hz, 1H), 6.94 (d, J=10.4 Hz, 2H), 3.81 (s, 3H).; MS (ESI) m/z 455 (M+H)+
 

Historical Records