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Chemical Structure| 1071017-64-5 Chemical Structure| 1071017-64-5

Structure of 1071017-64-5

Chemical Structure| 1071017-64-5

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Product Details of [ 1071017-64-5 ]

CAS No. :1071017-64-5
Formula : C11H16N2O
M.W : 192.26
SMILES Code : O=C(C1=C(C)C=NC=C1)NC(C)(C)C
MDL No. :MFCD24450267

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Application In Synthesis of [ 1071017-64-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1071017-64-5 ]

[ 1071017-64-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 7584-05-6 ]
  • [ 540-88-5 ]
  • [ 1071017-64-5 ]
YieldReaction ConditionsOperation in experiment
95% C. lambda/-f-Butyl-3-methy]isonicotinamide.; To the solution of the <strong>[7584-05-6]3-methyl-isonicotinonitrile</strong> (18.90 g, 159.92 mmol) in DCM (50 mL) is added f-BuOAc (72.63 mL, 538.84 mmol), followed by concentrated H2SO4 (12.32 mL, 874.46 mmol). The reaction is stirred for 8 h at rt, then diluted with a solution of saturated aqueous NaHCO3 and DCM (50 mL). The organic layer is washed with H2O, brine, dried over anhydrous Na2SO4 and then evaporated under reduced pressure to provide a white solid (29.30 g, 152.44 mmol, 95%).
  • 2
  • [ 1071017-64-5 ]
  • [ 1071017-49-6 ]
 

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