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Chemical Structure| 10537-63-0 Chemical Structure| 10537-63-0

Structure of 10537-63-0

Chemical Structure| 10537-63-0

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Product Details of [ 10537-63-0 ]

CAS No. :10537-63-0
Formula : C10H10O
M.W : 146.19
SMILES Code : CC(C1=CC=C(C=C)C=C1)=O
MDL No. :MFCD09033342
InChI Key :HDXVSRDSYNPSAE-UHFFFAOYSA-N
Pubchem ID :10909702

Safety of [ 10537-63-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 10537-63-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10537-63-0 ]

[ 10537-63-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 13329-40-3 ]
  • [ 60111-52-6 ]
  • [ 10537-63-0 ]
  • 2
  • [ 10537-63-0 ]
  • [ 201230-82-2 ]
  • [ 39105-51-6 ]
  • [ 41387-29-5 ]
YieldReaction ConditionsOperation in experiment
With water; toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; In butanone; at 114.84℃; under 40504.1 Torr; for 12.0h;Autoclave;Catalytic behavior; Kinetics; Carbonylation2 reactions were carried out in a 50 mL Parr autoclave reactor made of Hastelloy C-276 material following a procedure similar to that described previously [8]. For a typical reaction, the solid catalyst and the liquid phase reactants/solvent were charged in the reactor and sealed. The contents were heated to the desired temperature, then CO gas was introduced to the reactor to the desired pressure and the reaction started by switching on the stirring. The consumed CO was made up from a reservoir through a constant pressure regulator. The progress of the reaction was followed by observing the pressure drop in a CO reservoir as a function of time and the reaction was stopped at completion of CO absorption. Afterwards, the reactor was brought to ambient temperature, its content-gas was released and flushed thrice with N2 and liquid phase samples were analyzed for reactant/products composition using HP GC 6890 fitted with a HP-FFAP capillary column (25 m × 0.33 mm × 0.2 μm). GC-MS analyses of the samples were performed using Agilent 5973 N Mass Selective Detector attachment.
 

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