Home Cart Sign in  
Chemical Structure| 103804-80-4 Chemical Structure| 103804-80-4

Structure of 103804-80-4

Chemical Structure| 103804-80-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 103804-80-4 ]

CAS No. :103804-80-4
Formula : C6H11NO
M.W : 113.16
SMILES Code : N#CCC(C)(C)CO
MDL No. :MFCD07780281

Safety of [ 103804-80-4 ]

Application In Synthesis of [ 103804-80-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 103804-80-4 ]

[ 103804-80-4 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 1003-85-6 ]
  • [ 143-33-9 ]
  • [ 103804-80-4 ]
  • 2
  • [ 773837-37-9 ]
  • [ 1003-85-6 ]
  • [ 103804-80-4 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; In water; dimethyl sulfoxide; EXAMPLE 2 30 g (0.198 mol) of 5,5-dimethyl-1,3,2-dioxathiane 2-oxide (prepared in accordance with Example 1) and 15.5 g (0.317 mol) of dry, finely powdered NaCN in 40 ml of dry dimethyl sulphoxide are added while gassing with argon to a 350 ml four-necked flask which is provided with a stirrer, a reflux condenser and a thermometer. The reaction mixture is stirred at 100 C. for 30-36 hours. The majority of the dimethyl sulphoxide (35-36 ml) is then distilled off cautiously at 65-70 C./3 mmHg over a 5 cm Vigreux column. The residue is suspended in 130 ml of water and the suspension is brought to pH 3 with about 16 ml of 25% HCl solution. The black mixture is extracted continuously with 80 ml of isopropyl ether. After drying over Na2 SOt4 and removing the solvent on a rotary evaporator the product is distilled over a 5 cm Vigreux column at 75-82 C./0.2 mmHg. There are obtained 16 g of 4-hydroxy-3,3-dimethyl-butyronitrile in the form of an oil.
  • 3
  • [ 103804-80-4 ]
  • [ 156897-06-2 ]
 

Historical Records

Technical Information

Categories