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Chemical Structure| 103321-52-4 Chemical Structure| 103321-52-4

Structure of Fmoc-L-Pro-Cl
CAS No.: 103321-52-4

Chemical Structure| 103321-52-4

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Product Details of [ 103321-52-4 ]

CAS No. :103321-52-4
Formula : C20H18ClNO3
M.W : 355.81
SMILES Code : O=C(Cl)[C@H]1N(C(OCC2C3=CC=CC=C3C4=CC=CC=C24)=O)CCC1
MDL No. :MFCD00235831

Safety of [ 103321-52-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314
Precautionary Statements:P264-P270-P271-P280-P303+P361+P353-P304+P340-P305+P351+P338-P310-P330-P331-P363-P403+P233-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 103321-52-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 103321-52-4 ]

[ 103321-52-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 112253-70-0 ]
  • [ 103321-52-4 ]
  • (9H-fluoren-9-yl)methyl 2-(5-bromo-2-carbamoylphenylcarbamoyl)pyrrolidine-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In tetrahydrofuran; at 20℃; Example 5.25c. Synthesis of (9H-fluoren-9-yl)methyl 2-(5-bromo-2- carbamoylphenylcarbamovDpyrrolidine- 1 -carboxylateA solution of (9H-fluoren-9-yl)methyl 2-(chlorocarbonyl)pyrrolidine- l-carboxylate (600 mg, 1.8 mmol), <strong>[112253-70-0]2-amino-4-bromobenzamide</strong> (400 mg, 1.8 mmol), and Et3N (2 mL) in THF was stirred at room temperature . The reaction was monitored by TLC. After diluting with H20 (50 mL), the mixture was extracted with ethyl acetate (3 x 100 mL). The organic layers were dried over Na2S04 and concentrated to give yellow residue, which was purified by column chromatography. MS (ESI): 534, 536(MH+)
 

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