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Chemical Structure| 10316-79-7 Chemical Structure| 10316-79-7

Structure of 10316-79-7

Chemical Structure| 10316-79-7

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Product Details of [ 10316-79-7 ]

CAS No. :10316-79-7
Formula : C6H13NO
M.W : 115.17
SMILES Code : NC1(CO)CCCC1
MDL No. :MFCD00010491
InChI Key :PDNZJLMPXLQDPL-UHFFFAOYSA-N
Pubchem ID :66307

Safety of [ 10316-79-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 10316-79-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10316-79-7 ]

[ 10316-79-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 22280-60-0 ]
  • [ 10316-79-7 ]
  • [1-(6-methyl-5-nitro-pyridin-2-ylamino)-cyclopentyl]-methanol [ No CAS ]
YieldReaction ConditionsOperation in experiment
28% With triethylamine; In pentanol, 2-; at 180℃; for 2h;Microwave irradiation; Example 9 [1-(6-Methyl-5-nitro-pyridin-2-ylamino)-cyclopentyl]-methanol 6-Chloro-3-nitro-2-picoline (22 mg, 0.13 mmol) was coupled with (l-amino- cyclopentyl)-methanol (31 mg, 0.27 mmol), triethylamine (0.025 mL, 0.18 mmol) in 2- pentanol (1 mL). The reaction was heated to 180 °C for 2 h in a microwave oven (Parameters : high absorbance, fixed holding time, pre-stirring 25 seconds). The mixture was diluted with 20 mL of EtOAc and then washed with NaHCO3. The organic phase was collected, dried with anhydrous MgSO4 and filtered. The dry organic phase was evaporated and purified on a silica column with 5: 1 n-Heptane : EtOAc as mobile phase. This gave 9 mg (28percent) of [1-(6-methyl-5-nits-pyridin-2-ylamano)-cyclopentyl]- methanol as a yellow solid.
 

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