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Catalysts and Ligands
Transition metal
Ruthenium
RuCl[(R,R)-Fsdpen](p-cymene)
Catalysts and Ligands
Transition metal
Ruthenium

[ CAS No. 1026995-71-0 ] {[proInfo.proName]}

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Chemical Structure| 1026995-71-0
Chemical Structure| 1026995-71-0
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Quality Control of [ 1026995-71-0 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 1026995-71-0 ]

Product Details of [ 1026995-71-0 ]

CAS No. :1026995-71-0 MDL No. :MFCD12545953
Formula : C30H28ClF5N2O2RuS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 712.14 Pubchem ID :-
Synonyms :

Safety of [ 1026995-71-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P201-P202-P260-P264-P270-P281-P405-P501 UN#:N/A
Hazard Statements:H361-H371 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1026995-71-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1026995-71-0 ]

[ 1026995-71-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ CAS Unavailable ]
  • [ 1026785-12-5 ]
  • [ 1026995-71-0 ]
YieldReaction ConditionsOperation in experiment
With triethylamine In dichloromethane at 50℃; for 5h;
With triethylamine In dichloromethane for 5h; Reflux;
In tert-Amyl alcohol; chloroform at 55℃; for 0.5h; Inert atmosphere; ATH-DKR procedure for rac-α-acyl butyrolactone 2 - Synthesis of (S)-2-hydroxy-2-((S)-2-oxo-tetrahydrofuran-3-yl) ethyl benzoate (4) on 5 g scale A flame-dried RBF was charged with [RuCl2(p-cymene)]2 (245 mg, 0.40 mmol) and (R,R)-FSDPEN (354 mg, 0.80 mmol) in t-amyl alcohol (282 mL)-CHCl3 (121 mL). The RBF was purged with N2 and stirred at 55 °C for 30 min. After cooling to room temperature, compound 2 (5.0 g, 20.14 mmol) and formic acid:triethylamine (5:2) (21 mL) were added to the reaction mixture. The RBF was purged with N2, stirred at room temperature (27-30 °C) until the S5complete consumption of 2 as indicated by TLC. After the completion, the reaction was quenched by adding water and extracted with ethyl acetate. The organic layer was dried (Na2SO4) and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using petroleum ether as a mobile phase to yield 4.63 g (92% yield) of 4.
Reference： [1]Sun, Guodong; Zhou, Zihong; Luo, Zhonghua; Wang, Hailong; Chen, Lei; Xu, Yongbo; Li, Shun; Jian, Weilin; Zeng, Jiebin; Hu, Benquan; Han, Xiaodong; Lin, Yicao; Wang, Zhongqing [Organic Letters, 2017, vol. 19, # 16, p. 4339 - 4342]
[2]Luo, Zhonghua; Sun, Guodong; Zhou, Zihong; Liu, Guozhu; Luan, Baolei; Lin, Yicao; Zhang, Lei; Wang, Zhongqing [Chemical Communications, 2018, vol. 54, # 96, p. 13503 - 13506]
[3]More, Ganesh V.; Malekar, Pushpa V.; Kalshetti, Rupali G.; Shinde, Mahesh H.; Ramana, Chepuri V. [Tetrahedron Letters, 2021, vol. 66]

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[ 1026995-71-0 ]

Chemical Structure| 1026995-72-1

A903663[ 1026995-72-1 ]

Chloro{[(1S,2S)-(-)-2-amino-1,2-diphenylethyl](pentafluorophenylsulfonyl)amido}(p-cymene)ruthenium(II)

Reason: Optical isomers