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Chemical Structure| 10133-34-3 Chemical Structure| 10133-34-3

Structure of 10133-34-3

Chemical Structure| 10133-34-3

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Product Details of [ 10133-34-3 ]

CAS No. :10133-34-3
Formula : C8H5NO2S
M.W : 179.20
SMILES Code : O=[N+](C1=C(C=CS2)C2=CC=C1)[O-]

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Application In Synthesis of [ 10133-34-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10133-34-3 ]

[ 10133-34-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10133-34-3 ]
  • [ 17402-83-4 ]
YieldReaction ConditionsOperation in experiment
90% With 5%-palladium/activated carbon; hydrogen; In methanol; at 50℃; under 2250.23 Torr; for 6.5h;Autoclave; (a) Into a 500-mL autoclave, 80 g (0.446 mol) of 4-nitrobenzene[b]thiophene, 4 g (0.05 g/g) of 5percent palladium-carbon, and 320 mL of methanol were charged. After completion of the charging, the mixture was replaced with nitrogen three times, and then replaced with hydrogen. 3 times, charge hydrogen gas to a pressure of 0.3 MPa, stir, heat up at 50°C for 6 hours, keep the reaction until the kettle is no longer absorbing hydrogen, and then incubate the reaction for 30 minutes.After cooling down to room temperature, the reaction solution was taken out, suction-filtered under nitrogen, and the filtrate was concentrated under reduced pressure to a residual volume of 150 mL to give compound (II) with a weight of 60 g and a yield of 90percent.
 

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