Home Cart Sign in  
Chemical Structure| 101001-90-5 Chemical Structure| 101001-90-5

Structure of 101001-90-5

Chemical Structure| 101001-90-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 101001-90-5 ]

CAS No. :101001-90-5
Formula : C10H8N2O
M.W : 172.18
SMILES Code : O=C1C=CC=C(C2=NC=CC=C2)N1

Safety of [ 101001-90-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 101001-90-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 101001-90-5 ]

[ 101001-90-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 101001-90-5 ]
  • [ 13040-77-2 ]
YieldReaction ConditionsOperation in experiment
With trichlorophosphate; In ethyl acetate; A mixture of 5.3 g of 2-(2-pyridinyl)-6-(1H)-pyridinone and 100 ml of phosphorus oxychloride was heated on a steam bath for 18 hours and then concentrated to dryness under vacuum. Crushed ice was added to the oil residue and the mixture made basic with solid potassium carbonate. The mixture was then extracted with dichloromethane, the extracts treated with activated carbon, filtered and concentrated, giving a solid which was purified by chromatography on silica gel with ethyl acetate as solvent, giving 4.1 g of 6'-chloro-2,2'-bipyridine as white crystals, mp 60-62 C.
  • 2
  • [ 101001-90-5 ]
  • [ 101001-78-9 ]
  • [ 13040-77-2 ]
YieldReaction ConditionsOperation in experiment
In ethyl acetate; To 100 ml of phosphorus oxychloride, cooled in an ice bath, was added 5.3 g of [2,2'-bipyridin]-6(1H)-one. The mixture was warmed to room temperature and then heated on a steam bath for 18 hours, then concentrated under vacuum. Crushed ice was added to the residual oil and the solution was basified with solid potassium carbonate. This mixture was extracted with methylene chloride, the extract was dried and evaporated in vacuo to a solid This solid was dissolved in ethyl acetate and placed on a silica gel column. The column was eluted with ethyl acetate and the obtained solid recrystallized from heptane, giving 6'-chloro-2,2'-bipyridine as white crystals, mp 60-62 C., which was then treated as described in Example 1, giving the desired product.
  • 3
  • [ 110-86-1 ]
  • [ 52522-40-4 ]
  • [ 455-13-0 ]
  • [ 101001-90-5 ]
  • [Pd(bipy-6-O)(C6H4-p-CF3)(κ-N-py)] [ No CAS ]
 

Historical Records

Technical Information

Categories