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Chemical Structure| 10098-40-5 Chemical Structure| 10098-40-5

Structure of 10098-40-5

Chemical Structure| 10098-40-5

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Product Details of [ 10098-40-5 ]

CAS No. :10098-40-5
Formula : C9H9NO4
M.W : 195.17
SMILES Code : O=C(O)C1=CC=C(NC(C)=O)C(O)=C1
MDL No. :MFCD00869774

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Application In Synthesis of [ 10098-40-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10098-40-5 ]

[ 10098-40-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 136663-23-5 ]
  • [ 10098-40-5 ]
YieldReaction ConditionsOperation in experiment
100% Step 2: 2-Methylbenzord1oxazole-6-carboxyric acid (139); [0742] A solution of compound 138 (920 mg, 4.815 mmol) in THF: MeOH (30 mL of a 1 :1 solution) was treated with a solution of potassium hydroxide (0.698 g, 17.86 mmol) in H2O (15 mL). The reaction mixture was stirred for 65 min at room temperature then quenched with INHCl (18 mL, 18.6 mmol) (final pH of 2.5), THF was removed under reduced pressure and the remaining aqueous solution was cooled to -78 0C and lyophilized to give compound 139 (940 mg, quantitative).
 

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