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Chemical Structure| 1007171-35-8 Chemical Structure| 1007171-35-8

Structure of 1007171-35-8

Chemical Structure| 1007171-35-8

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Product Details of [ 1007171-35-8 ]

CAS No. :1007171-35-8
Formula : C11H14INO4S
M.W : 383.20
SMILES Code : O=C(C1=C(NC(OC(C)(C)C)=O)C=C(I)S1)OC
MDL No. :MFCD29762815

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Application In Synthesis of [ 1007171-35-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1007171-35-8 ]

[ 1007171-35-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1007171-35-8 ]
  • [ 942589-45-9 ]
YieldReaction ConditionsOperation in experiment
Intermediate 39Methyl 3-amino-5-iodo-2-thiophenecarboxylate <n="48"/>Intermediate 38 (4.097 g) was dissolved in 4M HCI in 1 ,4-dioxane solution (40 ml_). The resulting solution was stirred under nitrogen at room temperature for 7 h. The solvent was evaporated in vacuo and the residue was partitioned between saturated sodium bicarbonate solution and DCM. The organics were separated using a hydrophobic frit and were evaporated in vacuo to give the title compound. 1H NMR (CDCI3) delta 6.73 (1 H, s), 5.46 (2H, br), 3.82 (3H, s).
 

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