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Chemical Structure| 2390-59-2 Chemical Structure| 2390-59-2
Chemical Structure| 2390-59-2
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Product Details of Ethyl Violet

CAS No. :2390-59-2
Formula : C31H42ClN3
M.W : 492.14
SMILES Code : CC/[N+](CC)=C1C=C/C(C=C/1)=C(C2=CC=C(N(CC)CC)C=C2)\C3=CC=C(N(CC)CC)C=C3.[Cl-]
Synonyms :
Ethyl Violet
MDL No. :MFCD00011765
InChI Key :JVICFMRAVNKDOE-UHFFFAOYSA-M
Pubchem ID :16955

Safety of Ethyl Violet

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H361-H372-H410
Precautionary Statements:P201-P264-P280-P301+P330+P331-P312
Class:9
UN#:3077
Packing Group:

Application In Synthesis of Ethyl Violet

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2390-59-2 ]

[ 2390-59-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 135-91-1 ]
  • [ 91-66-7 ]
  • [ 2390-59-2 ]
YieldReaction ConditionsOperation in experiment
91.3% In a 250 mL reaction flask equipped with a thermometer, a reflux condenser, and a magnetic stirrer, 16.42 g (0.11 mol) was charged.N,N'-diethylaniline, 31.05g (0.1mol) 4,4'-bis (N,N'-diethyl)diphenylmethane (ethane bass), chloroform 100mL, Salen cobalt complex 0.5 g, 1.0 g of tetrachlorobenzoquinone, 10 mL of acetic acid, heated to 65 C with stirring, oxygen was flowed in, the flow rate was 18 mL / min, and the reaction was carried out for 6 hours.Sampling and analysis by HPLC showed that the conversion of the ethane bass reaction was complete. The reaction was stopped, and chloroform and acetic acid were distilled off.50 mL of water and 10 mL of concentrated hydrochloric acid were added, heated to 80 C., filtered, and the filtrate was cooled to room temperature, crystallized, and filtered to obtain crystals with metallic luster. After drying, weighed, 44.93 g, yield 91.3%. The characterization results are as follows:
 

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