Home Cart Sign in  
Chemical Structure| 99181-50-7 Chemical Structure| 99181-50-7

Structure of 99181-50-7

Chemical Structure| 99181-50-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 99181-50-7 ]

CAS No. :99181-50-7
Formula : C10H16O3
M.W : 184.23
SMILES Code : OC12CC3(O)CC(C2)(O)CC(C3)C1
MDL No. :MFCD08276262
InChI Key :MCYBYTIPMYLHAK-UHFFFAOYSA-N
Pubchem ID :9899022

Safety of [ 99181-50-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 99181-50-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 99181-50-7 ]

[ 99181-50-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 707-34-6 ]
  • [ 99181-50-7 ]
YieldReaction ConditionsOperation in experiment
210 g With sulfuric acid; water; silver sulfate; In toluene; at 110℃; for 16h; Step seven, equipped with a condenser, a thermometer four 5L reaction flask were successively added 473g1.3.5- tribromo adamantane, 946 g silver sulfate, 946 g of water and 94.6ml of toluene, stirring was started, 946 g of concentrated sulfuric acid was added dropwise, complete after the temperature was raised to about 110 deg.] C under reflux for 16 hours. (2 in the control) document.write(""); Step 8 After completion of the reaction, the temperature was lowered to room temperature, filtered, the filter cake was washed with 700ml of water and the combined filtrate, the filtrate was added 250g sodium bromide was stirred for half an hour excess silver ions precipitate was filtered, the filter cake was washed with 300ml of water, combined filtrate. The filtrate was diluted with 500ml of water was added.document.write(""); Step 9 using 30% sodium hydroxide solution PH = 12-13, at a temperature controlled above 75 , use up to about 2850 g of liquid caustic soda, After completion, it was cooled to 25-30 & deg.] C slowly, stirred for 30min, filtered, and collected by filtration cake. document.write(""); Step 10, the filter cake was added to 1.8L of methanol, 57g of activated carbon, stirred for IH, filtered, and the filtrate was recovered white paste, into 1.5L petroleum ether was filtered to give the product as a white solid 210g. (3 in the control)
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 99181-50-7 ]

Aliphatic Cyclic Hydrocarbons

Chemical Structure| 42822-86-6

A389939 [42822-86-6]

2-(2-Hydroxypropan-2-yl)-5-methylcyclohexanol

Similarity: 0.94

Chemical Structure| 10347-01-0

A388309 [10347-01-0]

5,7-Dimethyladamantane-1,3-diol

Similarity: 0.94

Chemical Structure| 10347-01-0

A388309 [10347-01-0]

5,7-Dimethyladamantane-1,3-diol

Similarity: 0.94

Chemical Structure| 17837-93-3

A413277 [17837-93-3]

5-Methyladamantane-1,3-diol

Similarity: 0.94

Chemical Structure| 474316-80-8

A124614 [474316-80-8]

1-Isopropylcyclohexane-1,3-diol

Similarity: 0.94

Alcohols

Chemical Structure| 42822-86-6

A389939 [42822-86-6]

2-(2-Hydroxypropan-2-yl)-5-methylcyclohexanol

Similarity: 0.94

Chemical Structure| 3564-98-5

A330174 [3564-98-5]

trans-2-(2-Hydroxypropan-2-yl)-5-methylcyclohexanol

Similarity: 0.94

Chemical Structure| 10347-01-0

A388309 [10347-01-0]

5,7-Dimethyladamantane-1,3-diol

Similarity: 0.94

Chemical Structure| 17837-93-3

A413277 [17837-93-3]

5-Methyladamantane-1,3-diol

Similarity: 0.94

Chemical Structure| 474316-80-8

A124614 [474316-80-8]

1-Isopropylcyclohexane-1,3-diol

Similarity: 0.94