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Chemical Structure| 944904-93-2 Chemical Structure| 944904-93-2

Structure of 944904-93-2

Chemical Structure| 944904-93-2

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Product Details of [ 944904-93-2 ]

CAS No. :944904-93-2
Formula : C11H7FN2O
M.W : 202.18
SMILES Code : O=CC1=CN=C(C2=CC=C(F)C=C2)N=C1

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Application In Synthesis of [ 944904-93-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 944904-93-2 ]

[ 944904-93-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 456-14-4 ]
  • 2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane bistetrafluoroborate [ No CAS ]
  • [ 944904-93-2 ]
YieldReaction ConditionsOperation in experiment
With ethanol; potassium tert-butylate; for 8h;Heating / reflux; Example 132 3-[2-(4-Fluoro-phenyl)-pyrimidin-5-yl]-N-(thiazol-2-yl)-acrylamide [Show Image] (a) 2-(4-Fluoro-phenyl)-pyrimidine-5-carbaldehyde; 2 g (11.45 mmol) of <strong>[456-14-4]4-fluorobenzamidine hydrochloride</strong>, 4.09 g (11.45 mmol) of 2-dimethylaminomethylene-1,3-bis(dimethylimmonio)propane-bis(tetrafluoroborate) and 3.86 g (34.36 mmol) of potassium tert-butylate in 70 ml of ethanol were heated under reflux for 8 h. After concentration, water and ethyl acetate were added. The organic phase was washed with a potassium hydrogensulfate solution and water, dried and evaporated. Yield: 1.87 g.
 

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