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Chemical Structure| 942070-18-0 Chemical Structure| 942070-18-0

Structure of 942070-18-0

Chemical Structure| 942070-18-0

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Product Details of [ 942070-18-0 ]

CAS No. :942070-18-0
Formula : C10H13BCl2O2S
M.W : 278.99
SMILES Code : CC1(C)C(C)(C)OB(C2=C(Cl)SC(Cl)=C2)O1
MDL No. :MFCD12405470
InChI Key :OZQVCTOZRVQPCE-UHFFFAOYSA-N
Pubchem ID :53429017

Safety of [ 942070-18-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 942070-18-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 942070-18-0 ]

[ 942070-18-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 128-09-6 ]
  • [ 214360-70-0 ]
  • [ 942070-18-0 ]
  • 2
  • [ 214360-70-0 ]
  • [ 942070-18-0 ]
YieldReaction ConditionsOperation in experiment
66% With N-chloro-succinimide; In N,N-dimethyl-formamide; at 20℃; for 14h; General procedure: To a solution of 3-anisyl pinacol borane (50mg, 0.21mmol) in DMF (1mL) was added N-bromosuccinimide (82mg, 0.46mmol). After stirring at room temperature for 14h, resultant solution was treated with 10% Na2S2O3 aq (10 ml) and was extracted with Et2O (10ml×3). The combined organic phase was washed with H2O (10ml×2) and brine (10ml×1) and dried over MgSO4. After removal of solvent under reduced pressure, the residue was chromatographed on silica gel with Hexane to afford 2-bromo-5-methoxyphenyl pinacol borate (57.3mg, 87% yield) as colorless oil
 

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