Home Cart Sign in  
Chemical Structure| 932702-42-6 Chemical Structure| 932702-42-6

Structure of 932702-42-6

Chemical Structure| 932702-42-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 932702-42-6 ]

CAS No. :932702-42-6
Formula : C16H21NO3
M.W : 275.34
SMILES Code : O=C(N1CC(OCC2CC2)CC1)OCC3=CC=CC=C3

Safety of [ 932702-42-6 ]

Application In Synthesis of [ 932702-42-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 932702-42-6 ]

[ 932702-42-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 95656-88-5 ]
  • [ 7051-34-5 ]
  • [ 932702-42-6 ]
YieldReaction ConditionsOperation in experiment
81% Sodium hydride (280 mmol) was added in portions to a cold (0 C.) solution of <strong>[95656-88-5]benzyl 3-hydroxypyrrolidine-1-carboxylate</strong> (76.9 mmol) in N,N-dimethylformamide (100 mL). The mixture was maintained for 60 min and was then treated with a solution of (bromomethyl)cyclopropane (231 mmol) in N,N-dimethylformamide (100 mL) and potassium iodide (0.66 mmol). The reaction mixture was allowed to warm to rt where it was maintained for 30 min. The reaction mixture was subjected to microwave irradiation for 2 h at 90 C. The reaction mixture was concentrated and the residue was diluted with ethyl acetate (200 mL) and water (200 mL) and the layers were separated. The aqueous layer was extracted with ethyl acetate (3*200 mL) and the combined organic layers were washed with brine (2*200 mL) and dried (magnesium sulfate). The residue was purified by chromatography (20/1 petroleum ether/ethyl acetate) to provide the product in 81% yield.
 

Historical Records