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Chemical Structure| 929973-95-5 Chemical Structure| 929973-95-5

Structure of 929973-95-5

Chemical Structure| 929973-95-5

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Product Details of [ 929973-95-5 ]

CAS No. :929973-95-5
Formula : C5H8N4
M.W : 124.14
SMILES Code : NC1N=C(CN)C=CN=1
MDL No. :MFCD09040794

Safety of [ 929973-95-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314
Precautionary Statements:P264-P270-P271-P280-P303+P361+P353-P304+P340-P305+P351+P338-P310-P330-P331-P363-P403+P233-P501
Class:8
UN#:3259
Packing Group:

Application In Synthesis of [ 929973-95-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 929973-95-5 ]

[ 929973-95-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 36314-98-4 ]
  • [ 929973-95-5 ]
YieldReaction ConditionsOperation in experiment
92% With ammonia; hydrogen; In methanol; at 20℃; under 24377.4 Torr; for 22.0h; Intermediate 1-11-4To a solution of <strong>[36314-98-4]2-aminopyrimidine-4-carbonitrile</strong> (1 g, 8.3 mmol) in 7M NH3 in MeOH (25.5 mL) was added Raney-Nickel (50% wet, 1.955 g, 33 mmol) and stirred at RT under an H2 atmosphere (32.5 bar) for 22h. The reaction was filtered and concentrated to give the intermediate 1-11-4 (954 mg, 92%) which was used without further purification.1H-NMR (400 MHz ,DMSO-d6), Shift [ppm]= 3.55 (2H), 6.34-6.54 (2H), 6.63 (1H), 8.09- 8.21 (1H).
 

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