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Structure of 917885-01-9

Chemical Structure| 917885-01-9

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Product Details of [ 917885-01-9 ]

CAS No. :917885-01-9
Formula : C9H7FO2
M.W : 166.15
SMILES Code : O=C1CCC2=C1C=C(O)C(F)=C2
MDL No. :MFCD09261203
InChI Key :YRHPPGLYOYCXOT-UHFFFAOYSA-N
Pubchem ID :44829108

Safety of [ 917885-01-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501

Application In Synthesis of [ 917885-01-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 917885-01-9 ]

[ 917885-01-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 83802-71-5 ]
  • [ 917885-01-9 ]
YieldReaction ConditionsOperation in experiment
With boron tribromide; In dichloromethane; at 20℃; for 7h;Cooling with ice; To an ice-cold solution of Compound III (666 mg) in methylene chloride (15 mL) was added dropwise boron tribromide (4.44 mL), and the mixture was stirred at room temperature for 7 hours. The reaction solution was cooled with ice, and thereto was added water, and the mixture was extracted with ethyl acetate. The organic layer was washed with brine, concentrated under reduced pressure, and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate=3/1) to give Compound III (52 mg).
 

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