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Chemical Structure| 878465-96-4 Chemical Structure| 878465-96-4

Structure of 878465-96-4

Chemical Structure| 878465-96-4

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Product Details of [ 878465-96-4 ]

CAS No. :878465-96-4
Formula : C8H9ClN2O2
M.W : 200.62
SMILES Code : O=C(NN)C1=CC=C(Cl)C=C1OC
MDL No. :MFCD08245268

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Application In Synthesis of [ 878465-96-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 878465-96-4 ]

[ 878465-96-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 78955-90-5 ]
  • [ 878465-96-4 ]
YieldReaction ConditionsOperation in experiment
73% With hydrazine; In methanol;Heating / reflux; (b) 4-Chloro-2-methoxybenzohydrazide. A mixture of methyl4-chloro-2-methoxybenzoate (6.0 g, 29.9 mmol), methanol (50 mL) and hydrazine hydrate (6.0 mL, 123.3 mmol) was refluxed overnight. The reaction mixture was cooled to room temperature and the precipitate was collected by filtration and further dried under vacuum to give the title compound as white solids (4.36 g, 21.7 mmol, 73%). 1H NMR (DMSO-d6): 9.24 (broad, s, IH)5 7.65 (d, IH, J = 8.4 Hz)3 7.19 (d, IH3 J = 2.1 Hz)3 7.08 (dd3 IH, J = 1.8, 8.1 Hz), 4.53 (d, 2H3 J= 4.2 Hz), 3.88 (s, 3H).
 

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