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Chemical Structure| 87476-69-5 Chemical Structure| 87476-69-5

Structure of 87476-69-5

Chemical Structure| 87476-69-5

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Product Details of [ 87476-69-5 ]

CAS No. :87476-69-5
Formula : C7H3BrClNO2S
M.W : 280.53
SMILES Code : ClC(C1=CC=C(Br)C=C12)=NS2(=O)=O

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Application In Synthesis of [ 87476-69-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 87476-69-5 ]

[ 87476-69-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 62473-92-1 ]
  • [ 87476-69-5 ]
YieldReaction ConditionsOperation in experiment
With phosphorus pentachloride; trichlorophosphate; at 160℃; for 16h; B. [1, 1-DIOXO-6-(3-TRIFLUOROMETHYL-PHENYL)1H-?6-BENZO[D]ISOTHIAZO-3-YL]-(4- TERT-BUTYL-PHENYL)-AMINE 1. 6-bromo-3-chloro-benzo[d]isothiazole 1,1-dioxide Heat a mixture of 6-bromo-1, 1-dioxo-1, 2-DIHYDRO-1 ? 6-benzo [d] isothiazol-3-one (Kwon et al. (1996) Arzneim. FORSCH. 46 (10): 966-971 ; 1.5 MMOL), POC13 (3 ml) and PCIS (2.0 mmol) for 16 hours at 160°C. Quench with ice, extract with EtOAc, and concentrate to give 6-bromo-3-chloro-benzo [d] isothiazole 1, 1-dioxide.
 

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