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Chemical Structure| 845973-23-1 Chemical Structure| 845973-23-1

Structure of 845973-23-1

Chemical Structure| 845973-23-1

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Product Details of [ 845973-23-1 ]

CAS No. :845973-23-1
Formula : C12H10BrNO
M.W : 264.12
SMILES Code : BrC1=NC=C(COC2=CC=CC=C2)C=C1

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Application In Synthesis of [ 845973-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 845973-23-1 ]

[ 845973-23-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 101990-45-8 ]
  • [ 108-95-2 ]
  • [ 845973-23-1 ]
YieldReaction ConditionsOperation in experiment
71% With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 90℃; for 2h; Example 17 Step 1: A mixture of the product from Example 16, Step 1 (0.70 g, 2.8 MMOL), phenol (0.19 g, 2.0 MMOL), and K2CO3 (0.58 g, 4.2 mmol) in anhydrous DMF (10 ml) was heated to 90 C for 2 h. The mixture was cooled down to RT, diluted with water, extracted with ether, dried (MGS04), filtered and concentrated. The residue was subjected to flash chromatography (5: 95 EtOAc/hexanes) to afford the product as white solid (0.38 g, 71 %).
 

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