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Chemical Structure| 84501-81-5 Chemical Structure| 84501-81-5

Structure of 84501-81-5

Chemical Structure| 84501-81-5

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Product Details of [ 84501-81-5 ]

CAS No. :84501-81-5
Formula : C2H3Cl3O2S
M.W : 197.47
SMILES Code : O=S(C(Cl)CCl)(Cl)=O
MDL No. :MFCD19200182

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Application In Synthesis of [ 84501-81-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 84501-81-5 ]

[ 84501-81-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6608-47-5 ]
  • [ 84501-81-5 ]
YieldReaction ConditionsOperation in experiment
31% With tetrachloromethane; at 20℃; for 5h;Irradiation; 1,2-Dichloroethanesulfonyl chloride. A stirred solution of chlorine in a solution of <strong>[6608-47-5]ethenesulfonyl chloride</strong> (32 g, 0.25 mol) in carbon tetrachloride was irradiated at about room temperature (200W light) for 5 h. The reaction mixture was concentrated under reduced pressure (50 mm Hg) and the involatile residue was fractionally distilled to give 1,2-dichloroethanesulfonyl chloride (Goldstein et al. Zh. Obshch. Khim., 28, 1958, 2107) (15,5 g, 31%), b. p. 75 C/0. 7 mm Hg. 1H-NMR (CDCl3) delta 5.29 (dd, J = 8.9 and 3.3 Hz, 1H), 4.40 (dd, J = 12.4 and 3.3 Hz, 1H), and 3.97 (dd, J = 12.4 and 8.9 Hz, 1H).
 

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