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Chemical Structure| 78826-46-7 Chemical Structure| 78826-46-7

Structure of 78826-46-7

Chemical Structure| 78826-46-7

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Product Details of [ 78826-46-7 ]

CAS No. :78826-46-7
Formula : C6H11ClO2
M.W : 150.60
SMILES Code : O=C(Cl)COC(C)(C)C
MDL No. :MFCD25967256

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Application In Synthesis of [ 78826-46-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 78826-46-7 ]

[ 78826-46-7 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 79-37-8 ]
  • [ 13211-32-0 ]
  • [ 78826-46-7 ]
YieldReaction ConditionsOperation in experiment
In N,N-dimethyl-formamide; toluene; (1,1-Dimethylethoxy)acetyl chloride To a 3-neck 500 ml round-bottom flask equipped with a magnetic stirrer, reflux condenser and addition funnel was added <strong>[13211-32-0](1,1-dimethylethoxy)acetic acid</strong> (24.00 g, 0.182 moles) and 300 ml of toluene under nitrogen. Oxalyl chloride (46.10 g, 0.363 moles) was then added dropwise and to this mixture was added N,N-dimethylformamide (0.25 g, 0.003 moles). This solution was heated at 30°-40° C. for 5 hours and then concentrated in vacuo to give 14.5 g of the product as a brown oil.
 

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